##TITLE=              31P MAS NMR spectrum of calcined STA-15
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Han et al. Chem. Mater., 22, 338-346 (2010) Figure 4
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/22 11:09:30
##SOURCE REFERENCE=   SAF-31P-Han-2010-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              SAF
##NAMES=              STA-15
##SAMPLE DESCRIPTION= STA-15, calcined

$$Bibliographic information 
##$AUTHORS=           Han, Z., Lorena Picone, A., Slawin, A.M., Seymour, V.R., Ashbrook, S.E., Zhou, W., Thompson, S.P., Parker, J.E., Wright, P.A.
##$TITLE=             Novel large-pore aluminophosphate molecular sieve STA-15 prepared using the tetrapropylammonium cation as a structure directing agent
##$JOURNAL=           Chemistry of Materials
##$VOLUME=            22
##$PAGES=             338-346
##$YEAR=              2010
##$DOI=               10.1021/cm902528y
##$FIGURE=            Figure 4

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         4
##$PEAK LABELS=        A          B          C          D         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -32.7435   -32.5435   -32.3435   -29.6783   
##$PEAK AREAS=         1.         1.         1.         1.        
##$PEAK WIDTHS=        3.71107    3.71107    3.71107    3.71107   
##$PEAK SHAPES=        0.48277    0.48277    0.48277    0.48277   
##$NUMBERING REF=     Han et al. Chem. Mater., 22, 338-346 (2010)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 243.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     10000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              4.3                  
##LASTX=              -54.5                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            197
##FIRSTY=             -0.00017              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  4.3                -0.00017              
  4                   0.00043              
  3.7                 0.00106              
  3.4                 0.00055              
  3.1                 0.00062              
  2.8                 0.00148              
  2.5                 0.00133              
  2.2                 0.00032              
  1.9                -0.00027              
  1.6                -0.00018              
  1.3                -0.00021              
  1.                 -0.00019              
  0.7                -0.00024              
  0.4                -0.00005              
  0.1                 0.00050              
 -0.2                 0.00041              
 -0.5                 0.00007              
 -0.8                 0.00058              
 -1.1                 0.00141              
 -1.4                 0.00108              
 -1.7                 0.00073              
 -2.                  0.00142              
 -2.3                 0.00099              
 -2.6                -0.00004              
 -2.9                -0.00020              
 -3.2                -0.00021              
 -3.5                -0.00018              
 -3.8                 0.00109              
 -4.1                 0.00226              
 -4.4                 0.00095              
 -4.7                -0.00012              
 -5.                 -0.00020              
 -5.3                -0.00020              
 -5.6                -0.00020              
 -5.9                -0.00020              
 -6.2                -0.00020              
 -6.5                -0.00020              
 -6.8                -0.00020              
 -7.1                -0.00020              
 -7.4                -0.00018              
 -7.7                -0.00025              
 -8.                 -0.00102              
 -8.3                -0.00176              
 -8.6                -0.00118              
 -8.9                -0.00030              
 -9.2                -0.00020              
 -9.5                -0.00020              
 -9.8                -0.00020              
 -10.1               -0.00020              
 -10.4               -0.00019              
 -10.7               -0.00025              
 -11.                 0.00001              
 -11.3                0.00129              
 -11.6                0.00180              
 -11.9                0.00097              
 -12.2                0.00000              
 -12.5               -0.00010              
 -12.8                0.00070              
 -13.1                0.00192              
 -13.4                0.00265              
 -13.7                0.00279              
 -14.                 0.00278              
 -14.3                0.00350              
 -14.6                0.00492              
 -14.9                0.00503              
 -15.2                0.00406              
 -15.5                0.00458              
 -15.8                0.00554              
 -16.1                0.00444              
 -16.4                0.00415              
 -16.7                0.00603              
 -17.                 0.00657              
 -17.3                0.00600              
 -17.6                0.00644              
 -17.9                0.00717              
 -18.2                0.00811              
 -18.5                0.00959              
 -18.8                0.01031              
 -19.1                0.01023              
 -19.4                0.01173              
 -19.7                0.01351              
 -20.                 0.01227              
 -20.3                0.01166              
 -20.6                0.01359              
 -20.9                0.01549              
 -21.2                0.01729              
 -21.5                0.01883              
 -21.8                0.01855              
 -22.1                0.01893              
 -22.4                0.02004              
 -22.7                0.02064              
 -23.                 0.02249              
 -23.3                0.02514              
 -23.6                0.02647              
 -23.9                0.02777              
 -24.2                0.03004              
 -24.5                0.03374              
 -24.8                0.03845              
 -25.1                0.04419              
 -25.4                0.05082              
 -25.7                0.05912              
 -26.                 0.06957              
 -26.3                0.08021              
 -26.6                0.09018              
 -26.9                0.10049              
 -27.2                0.11190              
 -27.5                0.12649              
 -27.8                0.14394              
 -28.1                0.16634              
 -28.4                0.19703              
 -28.7                0.22793              
 -29.                 0.26341              
 -29.3                0.29881              
 -29.6                0.33113              
 -29.9                0.36863              
 -30.2                0.40845              
 -30.5                0.45383              
 -30.8                0.50947              
 -31.1                0.56585              
 -31.4                0.61673              
 -31.7                0.65930              
 -32.                 0.68613              
 -32.3                0.69316              
 -32.6                0.67869              
 -32.9                0.64572              
 -33.2                0.60160              
 -33.5                0.54574              
 -33.8                0.47705              
 -34.1                0.40787              
 -34.4                0.33934              
 -34.7                0.27547              
 -35                  0.22092              
 -35.3                0.17313              
 -35.6                0.13586              
 -35.9                0.10677              
 -36.2                0.08067              
 -36.5                0.06246              
 -36.8                0.04639              
 -37.1                0.03373              
 -37.4                0.02670              
 -37.7                0.02249              
 -38.                 0.02064              
 -38.3                0.02005              
 -38.6                0.01825              
 -38.9                0.01516              
 -39.2                0.01393              
 -39.5                0.01403              
 -39.8                0.01276              
 -40.1                0.01078              
 -40.4                0.01018              
 -40.7                0.01027              
 -41.                 0.01014              
 -41.3                0.00868              
 -41.6                0.00660              
 -41.9                0.00593              
 -42.2                0.00632              
 -42.5                0.00699              
 -42.8                0.00627              
 -43.1                0.00571              
 -43.4                0.00577              
 -43.7                0.00579              
 -44.                 0.00563              
 -44.3                0.00454              
 -44.6                0.00326              
 -44.9                0.00333              
 -45.2                0.00452              
 -45.5                0.00375              
 -45.8                0.00264              
 -46.1                0.00279              
 -46.4                0.00287              
 -46.7                0.00369              
 -47.                 0.00524              
 -47.3                0.00564              
 -47.6                0.00453              
 -47.9                0.00312              
 -48.2                0.00308              
 -48.5                0.00461              
 -48.8                0.00485              
 -49.1                0.00353              
 -49.4                0.00269              
 -49.7                0.00280              
 -50.                 0.00277              
 -50.3                0.00278              
 -50.6                0.00278              
 -50.9                0.00278              
 -51.2                0.00278              
 -51.5                0.00278              
 -51.8                0.00278              
 -52.1                0.00277              
 -52.4                0.00280              
 -52.7                0.00270              
 -53.                 0.00191              
 -53.3                0.00112              
 -53.6                0.00153              
 -53.9                0.00253              
 -54.2                0.00282              
 -54.5                0.00270              
##END=
