##TITLE=              29Si CP MAS NMR spectrum of as-made pure silica Dodecasil-1H (with 1-aminoadamantane)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Groenen et al. Zeolites, 5, 361-363 (1985) Figure 1a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 14:20:13
##SOURCE REFERENCE=   DOH-29Si-Groenen-1985-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              DOH
##NAMES=              Dodecasil-1H
##SAMPLE DESCRIPTION= Dodecasil-1H, as-made

$$Bibliographic information 
##$AUTHORS=           Groenen, E.J., Alma, N.C., Dorrepaal, J., Hays, G.R., Kortbeek, A.G.
##$TITLE=             Solid-state 29Si n.m.r. spectroscopy of clathrasils; the relationship between the chemical shift and the structure of silicates
##$JOURNAL=           Zeolites
##$VOLUME=            5
##$PAGES=             361-363
##$YEAR=              1985
##$DOI=               10.1016/0144-2449(85)90126-5
##$FIGURE=            Figure 1a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         4
##$PEAK LABELS=        Si3        Si1/Si2    Si4        Si2/Si1       
##$PEAK TSITES=        T3         T1/T2      T4         T2/T1        
##$PEAK QTYPES=       
##$PEAK POSITIONS=    -121.151   -118.013   -117.699   -115.631   
##$PEAK AREAS=         3.         6.         2.         6.        
##$PEAK WIDTHS=        0.42783    0.5089     0.5089     0.43308   
##$PEAK SHAPES=        1          1          1          1         
##$NUMBERING REF=     Gies. J. Incl. Phenom. 4, 85-91 (1986)
##$ASSIGN REF=        Groenen et al. Zeolites, 5, 361-363 (1985) Table 1
##$ASSIGN METHOD=     relative intensities
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 
##.PULSE SEQUENCE=    cross polarization
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -106.06               
##LASTX=              -127.84               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            727
##FIRSTY=              0.10338              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -106.06              0.10338              
 -106.09              0.09518              
 -106.12              0.08534              
 -106.15              0.07841              
 -106.18              0.07593              
 -106.21              0.07649              
 -106.24              0.07514              
 -106.27              0.06916              
 -106.3               0.06367              
 -106.33              0.06308              
 -106.36              0.06408              
 -106.39              0.07010              
 -106.42              0.07525              
 -106.45              0.07847              
 -106.48              0.08271              
 -106.51              0.08425              
 -106.54              0.08399              
 -106.57              0.08410              
 -106.6               0.08407              
 -106.63              0.08409              
 -106.66              0.08408              
 -106.69              0.08410              
 -106.72              0.08404              
 -106.75              0.08425              
 -106.78              0.08237              
 -106.81              0.07433              
 -106.84              0.06850              
 -106.87              0.06849              
 -106.9               0.06829              
 -106.93              0.06997              
 -106.96              0.07294              
 -106.99              0.07543              
 -107.02              0.07643              
 -107.05              0.07622              
 -107.08              0.07628              
 -107.11              0.07629              
 -107.14              0.07622              
 -107.17              0.07650              
 -107.2               0.07484              
 -107.23              0.06973              
 -107.26              0.05929              
 -107.29              0.05315              
 -107.32              0.04994              
 -107.35              0.04394              
 -107.38              0.03910              
 -107.41              0.03645              
 -107.44              0.03982              
 -107.47              0.04527              
 -107.5               0.05067              
 -107.53              0.05328              
 -107.56              0.05275              
 -107.59              0.05289              
 -107.62              0.05280              
 -107.65              0.05311              
 -107.68              0.05202              
 -107.71              0.05892              
 -107.74              0.06863              
 -107.77              0.07727              
 -107.8               0.08497              
 -107.83              0.08979              
 -107.86              0.09232              
 -107.89              0.09180              
 -107.92              0.09192              
 -107.95              0.09189              
 -107.98              0.09190              
 -108.01              0.09187              
 -108.04              0.09202              
 -108.07              0.09146              
 -108.1               0.09487              
 -108.13              0.10015              
 -108.16              0.10830              
 -108.19              0.11616              
 -108.22              0.12096              
 -108.25              0.12356              
 -108.28              0.12304              
 -108.31              0.12314              
 -108.34              0.12314              
 -108.37              0.12301              
 -108.4               0.12201              
 -108.43              0.11072              
 -108.46              0.09616              
 -108.49              0.07720              
 -108.52              0.06258              
 -108.55              0.05483              
 -108.58              0.04764              
 -108.61              0.04867              
 -108.64              0.05209              
 -108.67              0.05086              
 -108.7               0.04595              
 -108.73              0.04708              
 -108.76              0.05126              
 -108.79              0.05653              
 -108.82              0.06507              
 -108.85              0.07043              
 -108.88              0.07438              
 -108.91              0.07619              
 -108.94              0.07880              
 -108.97              0.08349              
 -109.                0.08419              
 -109.03              0.08406              
 -109.06              0.08405              
 -109.09              0.08422              
 -109.12              0.08206              
 -109.15              0.07789              
 -109.18              0.07420              
 -109.21              0.07173              
 -109.24              0.07240              
 -109.27              0.07675              
 -109.3               0.08108              
 -109.33              0.08059              
 -109.36              0.07621              
 -109.39              0.07072              
 -109.42              0.06734              
 -109.45              0.06241              
 -109.48              0.06024              
 -109.51              0.06070              
 -109.54              0.06063              
 -109.57              0.06185              
 -109.6               0.06981              
 -109.63              0.07618              
 -109.66              0.07633              
 -109.69              0.07605              
 -109.72              0.07749              
 -109.75              0.08027              
 -109.78              0.08338              
 -109.81              0.08438              
 -109.84              0.08386              
 -109.87              0.08754              
 -109.9               0.09175              
 -109.93              0.09186              
 -109.96              0.09228              
 -109.99              0.08905              
 -110.02              0.08321              
 -110.05              0.07812              
 -110.08              0.07589              
 -110.11              0.07646              
 -110.14              0.07595              
 -110.17              0.07850              
 -110.2               0.08302              
 -110.23              0.08413              
 -110.26              0.08409              
 -110.29              0.08392              
 -110.32              0.08559              
 -110.35              0.08860              
 -110.38              0.09098              
 -110.41              0.09306              
 -110.44              0.09888              
 -110.47              0.10489              
 -110.5               0.11339              
 -110.53              0.11814              
 -110.56              0.11168              
 -110.59              0.11512              
 -110.62              0.12028              
 -110.65              0.12252              
 -110.68              0.12148              
 -110.71              0.11700              
 -110.74              0.11362              
 -110.77              0.10944              
 -110.8               0.10712              
 -110.83              0.10768              
 -110.86              0.10729              
 -110.89              0.10853              
 -110.92              0.11211              
 -110.95              0.12072              
 -110.98              0.12380              
 -111.01              0.12280              
 -111.04              0.12627              
 -111.07              0.13256              
 -111.1               0.13565              
 -111.13              0.13486              
 -111.16              0.13019              
 -111.19              0.12725              
 -111.22              0.12046              
 -111.25              0.11088              
 -111.28              0.10302              
 -111.31              0.09921              
 -111.34              0.09908              
 -111.37              0.10410              
 -111.4               0.11166              
 -111.43              0.11953              
 -111.46              0.12753              
 -111.49              0.13020              
 -111.52              0.13106              
 -111.55              0.13088              
 -111.58              0.13099              
 -111.61              0.13079              
 -111.64              0.13147              
 -111.67              0.12664              
 -111.7               0.11590              
 -111.73              0.10829              
 -111.76              0.09842              
 -111.79              0.09145              
 -111.82              0.09521              
 -111.85              0.09920              
 -111.88              0.10123              
 -111.91              0.10397              
 -111.94              0.10672              
 -111.97              0.10719              
 -112.                0.11001              
 -112.03              0.11434              
 -112.06              0.11637              
 -112.09              0.10917              
 -112.12              0.09805              
 -112.15              0.08969              
 -112.18              0.08410              
 -112.21              0.08419              
 -112.24              0.08367              
 -112.27              0.08685              
 -112.3               0.09272              
 -112.33              0.09756              
 -112.36              0.10147              
 -112.39              0.10292              
 -112.42              0.09992              
 -112.45              0.09542              
 -112.48              0.09825              
 -112.51              0.09982              
 -112.54              0.09950              
 -112.57              0.10142              
 -112.6               0.10589              
 -112.63              0.10779              
 -112.66              0.10740              
 -112.69              0.10753              
 -112.72              0.10750              
 -112.75              0.10751              
 -112.78              0.10751              
 -112.81              0.10751              
 -112.84              0.10751              
 -112.87              0.10750              
 -112.9               0.10753              
 -112.93              0.10738              
 -112.96              0.10793              
 -112.99              0.10440              
 -113.02              0.10026              
 -113.05              0.09833              
 -113.08              0.09461              
 -113.11              0.08607              
 -113.14              0.07858              
 -113.17              0.07206              
 -113.2               0.06784              
 -113.23              0.06816              
 -113.26              0.07122              
 -113.29              0.07941              
 -113.32              0.09380              
 -113.35              0.10560              
 -113.38              0.11571              
 -113.41              0.12324              
 -113.44              0.12293              
 -113.47              0.12365              
 -113.5               0.12051              
 -113.53              0.11633              
 -113.56              0.11298              
 -113.59              0.10858              
 -113.62              0.10745              
 -113.65              0.10756              
 -113.68              0.10750              
 -113.71              0.10750              
 -113.74              0.10754              
 -113.77              0.10738              
 -113.8               0.10876              
 -113.83              0.11333              
 -113.86              0.11576              
 -113.89              0.11504              
 -113.92              0.11627              
 -113.95              0.1211               
 -113.98              0.12661              
 -114.01              0.13249              
 -114.04              0.14261              
 -114.07              0.15083              
 -114.1               0.15670              
 -114.13              0.16323              
 -114.16              0.16960              
 -114.19              0.17467              
 -114.22              0.17640              
 -114.25              0.17969              
 -114.28              0.17962              
 -114.31              0.17577              
 -114.34              0.17843              
 -114.37              0.18763              
 -114.4               0.19522              
 -114.43              0.20140              
 -114.46              0.20749              
 -114.49              0.21608              
 -114.52              0.22078              
 -114.55              0.22926              
 -114.58              0.24167              
 -114.61              0.26435              
 -114.64              0.28279              
 -114.67              0.29836              
 -114.7               0.31779              
 -114.73              0.33242              
 -114.76              0.34424              
 -114.79              0.35269              
 -114.82              0.36895              
 -114.85              0.38791              
 -114.88              0.43635              
 -114.91              0.47680              
 -114.94              0.52796              
 -114.97              0.58305              
 -115.                0.66004              
 -115.03              0.74395              
 -115.06              0.85945              
 -115.09              0.98730              
 -115.12              1.0971               
 -115.15              1.2938               
 -115.18              1.47112              
 -115.21              1.77798              
 -115.24              2.07432              
 -115.27              2.39973              
 -115.3               2.75245              
 -115.33              3.32468              
 -115.36              3.78238              
 -115.39              4.41472              
 -115.42              5.13226              
 -115.45              5.65701              
 -115.48              6.40483              
 -115.51              7.13427              
 -115.54              7.77617              
 -115.57              8.18489              
 -115.6               8.49108              
 -115.63              8.71108              
 -115.66              8.48436              
 -115.69              8.19025              
 -115.72              7.56016              
 -115.75              7.02708              
 -115.78              6.47368              
 -115.81              5.79368              
 -115.84              5.0713               
 -115.87              4.43074              
 -115.9               3.95865              
 -115.93              3.39939              
 -115.96              3.03335              
 -115.99              2.68311              
 -116.02              2.34366              
 -116.05              2.10602              
 -116.08              1.87848              
 -116.11              1.66926              
 -116.14              1.49537              
 -116.17              1.34585              
 -116.2               1.19717              
 -116.23              1.13447              
 -116.26              1.05645              
 -116.29              0.99858              
 -116.32              0.92718              
 -116.35              0.86810              
 -116.38              0.81976              
 -116.41              0.77721              
 -116.44              0.73891              
 -116.47              0.70488              
 -116.5               0.65875              
 -116.53              0.61670              
 -116.56              0.60367              
 -116.59              0.58916              
 -116.62              0.58400              
 -116.65              0.58663              
 -116.68              0.59135              
 -116.71              0.59330              
 -116.74              0.59614              
 -116.77              0.59891              
 -116.8               0.59866              
 -116.83              0.60488              
 -116.86              0.61557              
 -116.89              0.63008              
 -116.92              0.64461              
 -116.95              0.65939              
 -116.98              0.69876              
 -117.01              0.74704              
 -117.04              0.82132              
 -117.07              0.88978              
 -117.1               0.97287              
 -117.13              1.0481               
 -117.16              1.17042              
 -117.19              1.28383              
 -117.22              1.41753              
 -117.25              1.56484              
 -117.28              1.72955              
 -117.31              1.88912              
 -117.34              2.07696              
 -117.37              2.33229              
 -117.4               2.52346              
 -117.43              2.6986               
 -117.46              2.85371              
 -117.49              3.105                
 -117.52              3.35646              
 -117.55              3.61994              
 -117.58              3.85439              
 -117.61              4.10462              
 -117.64              4.31898              
 -117.67              4.62338              
 -117.7               4.99537              
 -117.73              5.28221              
 -117.76              5.78903              
 -117.79              6.22908              
 -117.82              6.69534              
 -117.85              7.23534              
 -117.88              7.78208              
 -117.91              8.16163              
 -117.94              8.46003              
 -117.97              8.73653              
 -118.                8.72913              
 -118.03              8.6875               
 -118.06              8.27319              
 -118.09              7.75069              
 -118.12              7.24885              
 -118.15              6.70445              
 -118.18              6.10752              
 -118.21              5.34444              
 -118.24              4.8423               
 -118.27              4.2673               
 -118.3               3.70632              
 -118.33              3.34983              
 -118.36              3.02917              
 -118.39              2.72286              
 -118.42              2.41938              
 -118.45              2.22021              
 -118.48              2.04402              
 -118.51              1.87564              
 -118.54              1.65866              
 -118.57              1.52065              
 -118.6               1.41383              
 -118.63              1.31668              
 -118.66              1.21616              
 -118.69              1.13428              
 -118.72              1.08484              
 -118.75              1.03954              
 -118.78              1.01302              
 -118.81              0.99032              
 -118.84              0.97634              
 -118.87              0.94233              
 -118.9               0.90944              
 -118.93              0.87690              
 -118.96              0.84859              
 -118.99              0.81676              
 -119.02              0.78692              
 -119.05              0.76184              
 -119.08              0.74310              
 -119.11              0.72849              
 -119.14              0.71121              
 -119.17              0.68585              
 -119.2               0.65954              
 -119.23              0.63499              
 -119.26              0.61940              
 -119.29              0.61519              
 -119.32              0.61499              
 -119.35              0.61490              
 -119.38              0.61656              
 -119.41              0.61955              
 -119.44              0.62201              
 -119.47              0.62305              
 -119.5               0.62269              
 -119.53              0.62335              
 -119.56              0.62045              
 -119.59              0.61539              
 -119.62              0.60542              
 -119.65              0.58732              
 -119.68              0.57303              
 -119.71              0.55145              
 -119.74              0.53130              
 -119.77              0.52038              
 -119.8               0.51301              
 -119.83              0.50181              
 -119.86              0.48958              
 -119.89              0.47199              
 -119.92              0.45528              
 -119.95              0.45226              
 -119.98              0.45019              
 -120.01              0.44471              
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 -120.07              0.44813              
 -120.1               0.45038              
 -120.13              0.45118              
 -120.16              0.45103              
 -120.19              0.45109              
 -120.22              0.45109              
 -120.25              0.45103              
 -120.28              0.45125              
 -120.31              0.45084              
 -120.34              0.46224              
 -120.37              0.47799              
 -120.4               0.4975               
 -120.43              0.51498              
 -120.46              0.52122              
 -120.49              0.52179              
 -120.52              0.52118              
 -120.55              0.53972              
 -120.58              0.56165              
 -120.61              0.60045              
 -120.64              0.64407              
 -120.67              0.71284              
 -120.7               0.78502              
 -120.73              0.88636              
 -120.76              1.04554              
 -120.79              1.19013              
 -120.82              1.36464              
 -120.85              1.5163               
 -120.88              1.78159              
 -120.91              2.05714              
 -120.94              2.38647              
 -120.97              2.72603              
 -121.                3.13217              
 -121.03              3.44618              
 -121.06              3.80867              
 -121.09              4.18582              
 -121.12              4.33845              
 -121.15              4.44667              
 -121.18              4.42244              
 -121.21              4.20402              
 -121.24              3.94266              
 -121.27              3.54905              
 -121.3               3.19576              
 -121.33              2.76333              
 -121.36              2.38099              
 -121.39              2.002                
 -121.42              1.64339              
 -121.45              1.46057              
 -121.48              1.2842               
 -121.51              1.13631              
 -121.54              1.00594              
 -121.57              0.91496              
 -121.6               0.81063              
 -121.63              0.74184              
 -121.66              0.67511              
 -121.69              0.61000              
 -121.72              0.56506              
 -121.75              0.52365              
 -121.78              0.47718              
 -121.81              0.43810              
 -121.84              0.41017              
 -121.87              0.37582              
 -121.9               0.34676              
 -121.93              0.31520              
 -121.96              0.29191              
 -121.99              0.27832              
 -122.02              0.26969              
 -122.05              0.24737              
 -122.08              0.22008              
 -122.11              0.18666              
 -122.14              0.15907              
 -122.17              0.14284              
 -122.2               0.12945              
 -122.23              0.12338              
 -122.26              0.10965              
 -122.29              0.09568              
 -122.32              0.08125              
 -122.35              0.07019              
 -122.38              0.05647              
 -122.41              0.04522              
 -122.44              0.04501              
 -122.47              0.04498              
 -122.5               0.04530              
 -122.53              0.04407              
 -122.56              0.05010              
 -122.59              0.05915              
 -122.62              0.06106              
 -122.65              0.05913              
 -122.68              0.05380              
 -122.71              0.04369              
 -122.74              0.03538              
 -122.77              0.03089              
 -122.8               0.02957              
 -122.83              0.02675              
 -122.86              0.02142              
 -122.89              0.02512              
 -122.92              0.03600              
 -122.95              0.05304              
 -122.98              0.06271              
 -123.01              0.06874              
 -123.04              0.07590              
 -123.07              0.07216              
 -123.1               0.06338              
 -123.13              0.06165              
 -123.16              0.07026              
 -123.19              0.07597              
 -123.22              0.07767              
 -123.25              0.08054              
 -123.28              0.08312              
 -123.31              0.08431              
 -123.34              0.08390              
 -123.37              0.08485              
 -123.4               0.09027              
 -123.43              0.09238              
 -123.46              0.08991              
 -123.49              0.08518              
 -123.52              0.08495              
 -123.55              0.07616              
 -123.58              0.06603              
 -123.61              0.05305              
 -123.64              0.03631              
 -123.67              0.02546              
 -123.7               0.02085              
 -123.73              0.02183              
 -123.76              0.02155              
 -123.79              0.02163              
 -123.82              0.02160              
 -123.85              0.02164              
 -123.88              0.02149              
 -123.91              0.02203              
 -123.94              0.01858              
 -123.97              0.01418              
 -124.                0.01370              
 -124.03              0.01383              
 -124.06              0.01380              
 -124.09              0.01381              
 -124.12              0.01381              
 -124.15              0.01381              
 -124.18              0.01381              
 -124.21              0.01380              
 -124.24              0.01383              
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##END=
