##TITLE=              29Si MAS NMR spectrum of calcined pure silica Decadodecasil 3R zeolite (DDR)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Fyfe et al. Zeolites, 10, 278-282 (1990) Figure 2a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/06/20 12:31:24
##SOURCE REFERENCE=   DDR-29Si-Fyfe-1990
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              DDR
##NAMES=              DD3R
##NAMES=              Decadodecasil 3R
##SAMPLE DESCRIPTION= Decadodecasil 3R, calcined

$$Bibliographic information 
##$AUTHORS=           Fyfe, C., Gies, H., Feng, Y., Grondey, H.
##$TITLE=             Two-dimensional 29Si MAS n.m.r. investigation of the three-dimensional structure of zeolite DD3R
##$JOURNAL=           Zeolites
##$VOLUME=            10
##$PAGES=             278-282
##$YEAR=              1990
##$DOI=               10.1016/0144-2449(94)90140-6
##$FIGURE=            Figure 2a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         8
##$PEAK TSITES=        T6         T3         T4         T2         T1         T5         T1         T7        
##$PEAK LABELS=        Si6        Si3        Si4        Si2        Si1a       Si5        Si1b       Si7       
##$PEAK POSITIONS=    -122.617   -121.248   -119.152   -113.592   -113.472   -113.311   -112.705   -112.071   
##$PEAK AREAS=         1.         3.         3.         3.         3.         3.         3.         1.        
##$PEAK WIDTHS=        0.50125    0.47894    0.59971    0.35086    0.35086    0.35086    0.63016    0.63016   
##$PEAK SHAPES=        0.8378     0.8378     0.8378     0.8378     0.8378     0.8378     0.8378     0.8378    
##$NUMBERING REF=     Gies, Zeitschrift fur Kristallographie 175, 93-104 (1986)
##$ASSIGN REF=        Fyfe et al, Zeolites 10, 278-282 (1990)
##$ASSIGN METHOD=     2D correlation NMR

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 79.49
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -108.96               
##LASTX=              -125.02               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            804
##FIRSTY=              0.05991              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -108.96              0.05991              
 -108.98              0.05991              
 -109.                0.05991              
 -109.02              0.05991              
 -109.04              0.05991              
 -109.06              0.05991              
 -109.08              0.05991              
 -109.1               0.05991              
 -109.12              0.05991              
 -109.14              0.05991              
 -109.16              0.05991              
 -109.18              0.05991              
 -109.2               0.05991              
 -109.22              0.05991              
 -109.24              0.05991              
 -109.26              0.05991              
 -109.28              0.05991              
 -109.3               0.05991              
 -109.32              0.05991              
 -109.34              0.05991              
 -109.36              0.05991              
 -109.38              0.05991              
 -109.4               0.05991              
 -109.42              0.05991              
 -109.44              0.05991              
 -109.46              0.05991              
 -109.48              0.05991              
 -109.5               0.05991              
 -109.52              0.05991              
 -109.54              0.05991              
 -109.56              0.05991              
 -109.58              0.05991              
 -109.6               0.05991              
 -109.62              0.05991              
 -109.64              0.05991              
 -109.66              0.05991              
 -109.68              0.05991              
 -109.7               0.05991              
 -109.72              0.05991              
 -109.74              0.05991              
 -109.76              0.05991              
 -109.78              0.05991              
 -109.8               0.05991              
 -109.82              0.05991              
 -109.84              0.05991              
 -109.86              0.05991              
 -109.88              0.05991              
 -109.9               0.05991              
 -109.92              0.05991              
 -109.94              0.05991              
 -109.96              0.05991              
 -109.98              0.05991              
 -110.                0.05991              
 -110.02              0.05990              
 -110.04              0.05991              
 -110.06              0.05991              
 -110.08              0.05990              
 -110.1               0.05993              
 -110.12              0.05985              
 -110.14              0.06000              
 -110.16              0.05999              
 -110.18              0.05885              
 -110.2               0.06647              
 -110.22              0.08078              
 -110.24              0.09003              
 -110.26              0.08946              
 -110.28              0.08915              
 -110.3               0.08939              
 -110.32              0.08929              
 -110.34              0.08932              
 -110.36              0.08932              
 -110.38              0.08932              
 -110.4               0.08932              
 -110.42              0.08932              
 -110.44              0.08932              
 -110.46              0.08932              
 -110.48              0.08932              
 -110.5               0.08932              
 -110.52              0.08932              
 -110.54              0.08932              
 -110.56              0.08932              
 -110.58              0.08932              
 -110.6               0.08932              
 -110.62              0.08932              
 -110.64              0.08932              
 -110.66              0.08932              
 -110.68              0.08932              
 -110.7               0.08932              
 -110.72              0.08932              
 -110.74              0.08932              
 -110.76              0.08932              
 -110.78              0.08932              
 -110.8               0.08932              
 -110.82              0.08932              
 -110.84              0.08932              
 -110.86              0.08932              
 -110.88              0.08932              
 -110.9               0.08932              
 -110.92              0.08932              
 -110.94              0.08932              
 -110.96              0.08932              
 -110.98              0.08932              
 -111.                0.08932              
 -111.02              0.08932              
 -111.04              0.08932              
 -111.06              0.08932              
 -111.08              0.08932              
 -111.1               0.08932              
 -111.12              0.08932              
 -111.14              0.08932              
 -111.16              0.08932              
 -111.18              0.08932              
 -111.2               0.08931              
 -111.22              0.08933              
 -111.24              0.08934              
 -111.26              0.08910              
 -111.28              0.09013              
 -111.3               0.08730              
 -111.32              0.09175              
 -111.34              0.11674              
 -111.36              0.12039              
 -111.38              0.11879              
 -111.4               0.11693              
 -111.42              0.12076              
 -111.44              0.14611              
 -111.46              0.14679              
 -111.48              0.16222              
 -111.5               0.17850              
 -111.52              0.17906              
 -111.54              0.21527              
 -111.56              0.24296              
 -111.58              0.26332              
 -111.6               0.28944              
 -111.62              0.32754              
 -111.64              0.37693              
 -111.66              0.39746              
 -111.68              0.45250              
 -111.7               0.53744              
 -111.72              0.59083              
 -111.74              0.63613              
 -111.76              0.69964              
 -111.78              0.77832              
 -111.8               0.86146              
 -111.82              0.94288              
 -111.84              1.01479              
 -111.86              1.07388              
 -111.88              1.13752              
 -111.9               1.20881              
 -111.92              1.26505              
 -111.94              1.29781              
 -111.96              1.35799              
 -111.98              1.42944              
 -112.                1.4811               
 -112.02              1.51472              
 -112.04              1.53605              
 -112.06              1.5766               
 -112.08              1.62213              
 -112.1               1.65337              
 -112.12              1.67639              
 -112.14              1.68821              
 -112.16              1.70508              
 -112.18              1.73636              
 -112.2               1.77033              
 -112.22              1.80455              
 -112.24              1.8758               
 -112.26              1.92125              
 -112.28              1.9662               
 -112.3               2.05932              
 -112.32              2.16555              
 -112.34              2.25718              
 -112.36              2.37051              
 -112.38              2.50668              
 -112.4               2.63075              
 -112.42              2.73484              
 -112.44              2.85639              
 -112.46              2.9996               
 -112.48              3.12826              
 -112.5               3.24812              
 -112.52              3.41377              
 -112.54              3.55641              
 -112.56              3.65764              
 -112.58              3.75472              
 -112.6               3.87579              
 -112.62              3.99593              
 -112.64              4.07564              
 -112.66              4.13868              
 -112.68              4.18779              
 -112.7               4.20734              
 -112.72              4.22029              
 -112.74              4.21754              
 -112.76              4.18768              
 -112.78              4.13141              
 -112.8               4.05956              
 -112.82              3.98734              
 -112.84              3.93083              
 -112.86              3.85586              
 -112.88              3.75833              
 -112.9               3.67894              
 -112.92              3.6283               
 -112.94              3.60009              
 -112.96              3.58193              
 -112.98              3.6229               
 -113.                3.77206              
 -113.02              3.94644              
 -113.04              4.13921              
 -113.06              4.45992              
 -113.08              4.88403              
 -113.1               5.24186              
 -113.12              5.56402              
 -113.14              6.02435              
 -113.16              6.72656              
 -113.18              7.43624              
 -113.2               7.904                
 -113.22              8.52501              
 -113.24              8.97641              
 -113.26              9.44939              
 -113.28              10.1645              
 -113.3               10.7283              
 -113.32              11.0682              
 -113.34              11.5795              
 -113.36              12.2827              
 -113.38              12.8368              
 -113.4               13.0804              
 -113.42              13.2475              
 -113.44              13.5669              
 -113.46              13.8644              
 -113.48              13.8569              
 -113.5               13.6282              
 -113.52              13.4383              
 -113.54              13.0305              
 -113.56              12.4117              
 -113.58              11.869               
 -113.6               11.3822              
 -113.62              10.7118              
 -113.64              9.78328              
 -113.66              8.93678              
 -113.68              8.3669               
 -113.7               7.64349              
 -113.72              6.83557              
 -113.74              6.13781              
 -113.76              5.53747              
 -113.78              4.9132               
 -113.8               4.33133              
 -113.82              3.91469              
 -113.84              3.51395              
 -113.86              3.16485              
 -113.88              3.00582              
 -113.9               2.7599               
 -113.92              2.4813               
 -113.94              2.30719              
 -113.96              2.16848              
 -113.98              1.9385               
 -114.                1.78411              
 -114.02              1.68469              
 -114.04              1.59317              
 -114.06              1.47655              
 -114.08              1.33394              
 -114.1               1.2457               
 -114.12              1.16751              
 -114.14              1.08941              
 -114.16              1.03998              
 -114.18              1.00655              
 -114.2               0.93680              
 -114.22              0.88695              
 -114.24              0.85367              
 -114.26              0.80330              
 -114.28              0.75599              
 -114.3               0.72805              
 -114.32              0.71231              
 -114.34              0.67263              
 -114.36              0.61456              
 -114.38              0.59214              
 -114.4               0.56888              
 -114.42              0.55255              
 -114.44              0.53918              
 -114.46              0.51382              
 -114.48              0.4898               
 -114.5               0.47559              
 -114.52              0.46680              
 -114.54              0.45023              
 -114.56              0.42670              
 -114.58              0.41515              
 -114.6               0.40204              
 -114.62              0.39869              
 -114.64              0.39441              
 -114.66              0.36808              
 -114.68              0.34229              
 -114.7               0.33909              
 -114.72              0.33430              
 -114.74              0.32307              
 -114.76              0.32459              
 -114.78              0.32584              
 -114.8               0.31680              
 -114.82              0.30420              
 -114.84              0.29222              
 -114.86              0.28070              
 -114.88              0.27962              
 -114.9               0.28203              
 -114.92              0.27625              
 -114.94              0.26334              
 -114.96              0.25181              
 -114.98              0.23896              
 -115.                0.23526              
 -115.02              0.23672              
 -115.04              0.23631              
 -115.06              0.23635              
 -115.08              0.23650              
 -115.1               0.23593              
 -115.12              0.23747              
 -115.14              0.23499              
 -115.16              0.22241              
 -115.18              0.22226              
 -115.2               0.21460              
 -115.22              0.20540              
 -115.24              0.20710              
 -115.26              0.20681              
 -115.28              0.20854              
 -115.3               0.19953              
 -115.32              0.19164              
 -115.34              0.19163              
 -115.36              0.17910              
 -115.38              0.17641              
 -115.4               0.17799              
 -115.42              0.17744              
 -115.44              0.17756              
 -115.46              0.17756              
 -115.48              0.17754              
 -115.5               0.17756              
 -115.52              0.17754              
 -115.54              0.17756              
 -115.56              0.17763              
 -115.58              0.17713              
 -115.6               0.17886              
 -115.62              0.17487              
 -115.64              0.16273              
 -115.66              0.16226              
 -115.68              0.16318              
 -115.7               0.16273              
 -115.72              0.16287              
 -115.74              0.16285              
 -115.76              0.16284              
 -115.78              0.16285              
 -115.8               0.16284              
 -115.82              0.16285              
 -115.84              0.16285              
 -115.86              0.16282              
 -115.88              0.16296              
 -115.9               0.16254              
 -115.92              0.16331              
 -115.94              0.16327              
 -115.96              0.15136              
 -115.98              0.14674              
 -116.                0.14856              
 -116.02              0.14807              
 -116.04              0.14813              
 -116.06              0.14816              
 -116.08              0.14813              
 -116.1               0.14814              
 -116.12              0.14814              
 -116.14              0.14814              
 -116.16              0.14814              
 -116.18              0.14814              
 -116.2               0.14814              
 -116.22              0.14814              
 -116.24              0.14814              
 -116.26              0.14814              
 -116.28              0.14814              
 -116.3               0.14814              
 -116.32              0.14814              
 -116.34              0.14814              
 -116.36              0.14814              
 -116.38              0.14814              
 -116.4               0.14814              
 -116.42              0.14814              
 -116.44              0.14814              
 -116.46              0.14814              
 -116.48              0.14814              
 -116.5               0.14814              
 -116.52              0.14814              
 -116.54              0.14814              
 -116.56              0.14814              
 -116.58              0.14814              
 -116.6               0.14814              
 -116.62              0.14814              
 -116.64              0.14814              
 -116.66              0.14814              
 -116.68              0.14814              
 -116.7               0.14814              
 -116.72              0.14814              
 -116.74              0.14814              
 -116.76              0.14813              
 -116.78              0.14816              
 -116.8               0.14810              
 -116.82              0.14812              
 -116.84              0.14851              
 -116.86              0.14658              
 -116.88              0.15301              
 -116.9               0.16391              
 -116.92              0.16299              
 -116.94              0.16263              
 -116.96              0.16295              
 -116.98              0.16281              
 -117.                0.16285              
 -117.02              0.16285              
 -117.04              0.16284              
 -117.06              0.16287              
 -117.08              0.16277              
 -117.1               0.16293              
 -117.12              0.16304              
 -117.14              0.16132              
 -117.16              0.17015              
 -117.18              0.17907              
 -117.2               0.17736              
 -117.22              0.17746              
 -117.24              0.17762              
 -117.26              0.17752              
 -117.28              0.17756              
 -117.3               0.17755              
 -117.32              0.17754              
 -117.34              0.17758              
 -117.36              0.17744              
 -117.38              0.17778              
 -117.4               0.17741              
 -117.42              0.17638              
 -117.44              0.18772              
 -117.46              0.19247              
 -117.48              0.19478              
 -117.5               0.20721              
 -117.52              0.20746              
 -117.54              0.20703              
 -117.56              0.20582              
 -117.58              0.20946              
 -117.6               0.22173              
 -117.62              0.22262              
 -117.64              0.21975              
 -117.66              0.2273               
 -117.68              0.23758              
 -117.7               0.23641              
 -117.72              0.23619              
 -117.74              0.23649              
 -117.76              0.23628              
 -117.78              0.23648              
 -117.8               0.23643              
 -117.82              0.23534              
 -117.84              0.24317              
 -117.86              0.25741              
 -117.88              0.26664              
 -117.9               0.26599              
 -117.92              0.26458              
 -117.94              0.27221              
 -117.96              0.28671              
 -117.98              0.29561              
 -118.                0.29489              
 -118.02              0.30463              
 -118.04              0.31881              
 -118.06              0.32627              
 -118.08              0.32381              
 -118.1               0.32296              
 -118.12              0.34655              
 -118.14              0.35532              
 -118.16              0.35745              
 -118.18              0.36907              
 -118.2               0.36753              
 -118.22              0.38793              
 -118.24              0.40708              
 -118.26              0.41624              
 -118.28              0.42859              
 -118.3               0.44045              
 -118.32              0.45064              
 -118.34              0.46903              
 -118.36              0.49401              
 -118.38              0.51703              
 -118.4               0.54020              
 -118.42              0.56523              
 -118.44              0.58192              
 -118.46              0.59304              
 -118.48              0.61996              
 -118.5               0.66911              
 -118.52              0.68937              
 -118.54              0.69970              
 -118.56              0.73269              
 -118.58              0.78062              
 -118.6               0.82467              
 -118.62              0.894                
 -118.64              0.94734              
 -118.66              0.98234              
 -118.68              1.04369              
 -118.7               1.104                
 -118.72              1.1554               
 -118.74              1.23702              
 -118.76              1.3459               
 -118.78              1.42485              
 -118.8               1.47537              
 -118.82              1.59119              
 -118.84              1.69862              
 -118.86              1.7901               
 -118.88              1.9722               
 -118.9               2.12969              
 -118.92              2.20353              
 -118.94              2.31237              
 -118.96              2.52014              
 -118.98              2.70779              
 -119.                2.80659              
 -119.02              2.92302              
 -119.04              3.10725              
 -119.06              3.28324              
 -119.08              3.37392              
 -119.1               3.45433              
 -119.12              3.534                
 -119.14              3.59138              
 -119.16              3.60197              
 -119.18              3.56452              
 -119.2               3.54112              
 -119.22              3.44132              
 -119.24              3.29641              
 -119.26              3.20045              
 -119.28              3.10033              
 -119.3               2.91853              
 -119.32              2.70936              
 -119.34              2.54606              
 -119.36              2.42075              
 -119.38              2.26993              
 -119.4               2.10539              
 -119.42              1.94644              
 -119.44              1.79909              
 -119.46              1.69063              
 -119.48              1.64883              
 -119.5               1.54155              
 -119.52              1.40821              
 -119.54              1.3219               
 -119.56              1.26585              
 -119.58              1.19705              
 -119.6               1.1226               
 -119.62              1.06383              
 -119.64              1.02091              
 -119.66              0.97320              
 -119.68              0.91305              
 -119.7               0.87077              
 -119.72              0.83828              
 -119.74              0.80317              
 -119.76              0.76805              
 -119.78              0.72038              
 -119.8               0.68623              
 -119.82              0.67429              
 -119.84              0.65749              
 -119.86              0.62078              
 -119.88              0.60824              
 -119.9               0.58711              
 -119.92              0.57378              
 -119.94              0.57224              
 -119.96              0.54679              
 -119.98              0.54582              
 -120.                0.53266              
 -120.02              0.50821              
 -120.04              0.50103              
 -120.06              0.50176              
 -120.08              0.49058              
 -120.1               0.48483              
 -120.12              0.48676              
 -120.14              0.48634              
 -120.16              0.48641              
 -120.18              0.48596              
 -120.2               0.48780              
 -120.22              0.48295              
 -120.24              0.47122              
 -120.26              0.47152              
 -120.28              0.47027              
 -120.3               0.47831              
 -120.32              0.48705              
 -120.34              0.48664              
 -120.36              0.49891              
 -120.38              0.50267              
 -120.4               0.49959              
 -120.42              0.50334              
 -120.44              0.51605              
 -120.46              0.52797              
 -120.48              0.53871              
 -120.5               0.55310              
 -120.52              0.55916              
 -120.54              0.55978              
 -120.56              0.59534              
 -120.58              0.61487              
 -120.6               0.62620              
 -120.62              0.65656              
 -120.64              0.69153              
 -120.66              0.70314              
 -120.68              0.72703              
 -120.7               0.77458              
 -120.72              0.81513              
 -120.74              0.83714              
 -120.76              0.89319              
 -120.78              0.94763              
 -120.8               0.98958              
 -120.82              1.04083              
 -120.84              1.11213              
 -120.86              1.19307              
 -120.88              1.28136              
 -120.9               1.41752              
 -120.92              1.53273              
 -120.94              1.5612               
 -120.96              1.78588              
 -120.98              1.97725              
 -121.                2.05989              
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##END=
