##TITLE=              31P MAS NMR spectrum of dehydrated AlPO-25 (formed by calcination of AlPO-21)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Jelinek et al. J. Am. Chem. Soc., 113, 4097-4101 (1991) Figure 6a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/20 06:37:49
##SOURCE REFERENCE=   ATV-31P-Jelinek-1991-dehydrated
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              ATV
##NAMES=              AlPO-25
##SAMPLE DESCRIPTION= AlPO-25, dehydrated

$$Bibliographic information 
##$AUTHORS=           Jelinek, R., Chmelka, B.F., Wu, Y., Grandinetti, P.J., Pines, A., Barrie, P.J., Klinowski, J.
##$TITLE=             Study of the Aluminophosphates AlPO4-21 and AlPO4-25 by 27Al Double-Rotation NMR
##$JOURNAL=           Journal of the American Chemical Society
##$VOLUME=            113
##$PAGES=             4097-4101
##$YEAR=              1991
##$DOI=               10.1021/ja00011a007
##$FIGURE=            Figure 6a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         2
##$PEAK LABELS=        P1         P2        
##$PEAK TSITES=        T1         T2        
##$PEAK POSITIONS=    -30.1475   -27.4535   
##$PEAK AREAS=         2.         1.        
##$PEAK WIDTHS=        3.78888    3.78888   
##$PEAK SHAPES=        0.17934    0.17934   
##$NUMBERING REF=     Richardson et al. J. Phys. Chem., 94, 3365-3367 (1990)
##$ASSIGN REF=        Jelinek et al. J. Am. Chem. Soc., 113, 4097-4101 (1991) Figure 6a
##$ASSIGN METHOD=     single peak
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 201.84
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     5500

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -0.6                  
##LASTX=              -59.4                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            295
##FIRSTY=             -0.00567              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -0.6                -0.00567              
 -0.8                -0.00567              
 -1                  -0.00569              
 -1.2                -0.00552              
 -1.4                -0.00443              
 -1.6                -0.00339              
 -1.8                -0.00290              
 -2.                 -0.00212              
 -2.2                -0.00132              
 -2.4                -0.00048              
 -2.6                 0.00026              
 -2.8                 0.00124              
 -3.                  0.00241              
 -3.2                 0.00374              
 -3.4                 0.00502              
 -3.6                 0.00580              
 -3.8                 0.00673              
 -4                   0.00800              
 -4.2                 0.00893              
 -4.4                 0.00978              
 -4.6                 0.01151              
 -4.8                 0.01286              
 -5.                  0.01288              
 -5.2                 0.01381              
 -5.4                 0.01458              
 -5.6                 0.01531              
 -5.8                 0.01573              
 -6                   0.01564              
 -6.2                 0.01568              
 -6.4                 0.01552              
 -6.6                 0.01399              
 -6.8                 0.01294              
 -7.                  0.01280              
 -7.2                 0.01161              
 -7.4                 0.00964              
 -7.6                 0.00831              
 -7.8                 0.00479              
 -8.                  0.00226              
 -8.2                 0.00049              
 -8.4                -0.00159              
 -8.6                -0.00292              
 -8.8                -0.00428              
 -9                  -0.00722              
 -9.2                -0.00944              
 -9.4                -0.00910              
 -9.6                -0.00955              
 -9.8                -0.01042              
 -10.                -0.01142              
 -10.2               -0.01210              
 -10.4               -0.01206              
 -10.6               -0.01207              
 -10.8               -0.01211              
 -11.                -0.01191              
 -11.2               -0.01146              
 -11.4               -0.01096              
 -11.6               -0.01063              
 -11.8               -0.01066              
 -12.                -0.01064              
 -12.2               -0.01067              
 -12.4               -0.01062              
 -12.6               -0.00996              
 -12.8               -0.00923              
 -13.                -0.00924              
 -13.2               -0.00921              
 -13.4               -0.00931              
 -13.6               -0.00887              
 -13.8               -0.00777              
 -14.                -0.00652              
 -14.2               -0.00566              
 -14.4               -0.00569              
 -14.6               -0.00565              
 -14.8               -0.00576              
 -15.                -0.00636              
 -15.2               -0.00700              
 -15.4               -0.00702              
 -15.6               -0.00714              
 -15.8               -0.00931              
 -16.                -0.01081              
 -16.2               -0.01043              
 -16.4               -0.00914              
 -16.6               -0.00769              
 -16.8               -0.00725              
 -17.                -0.00707              
 -17.2               -0.00726              
 -17.4               -0.00866              
 -17.6               -0.00931              
 -17.8               -0.00921              
 -18.                -0.00923              
 -18.2               -0.00923              
 -18.4               -0.00924              
 -18.6               -0.00914              
 -18.8               -0.00784              
 -19.                -0.00604              
 -19.2               -0.00503              
 -19.4               -0.00460              
 -19.6               -0.00424              
 -19.8               -0.00423              
 -20.                -0.00371              
 -20.2               -0.00271              
 -20.4               -0.00169              
 -20.6               -0.00097              
 -20.8                0.00024              
 -21.                 0.00190              
 -21.2                0.00386              
 -21.4                0.00557              
 -21.6                0.00769              
 -21.8                0.00920              
 -22.                 0.01036              
 -22.2                0.01193              
 -22.4                0.01376              
 -22.6                0.01831              
 -22.8                0.02305              
 -23.                 0.02533              
 -23.2                0.02874              
 -23.4                0.03295              
 -23.6                0.03623              
 -23.8                0.04121              
 -24.                 0.04923              
 -24.2                0.05786              
 -24.4                0.06944              
 -24.6                0.08159              
 -24.8                0.08996              
 -25.                 0.10231              
 -25.2                0.11796              
 -25.4                0.13338              
 -25.6                0.14361              
 -25.8                0.15962              
 -26.                 0.18296              
 -26.2                0.20099              
 -26.4                0.22304              
 -26.6                0.24686              
 -26.8                0.25870              
 -27.                 0.27554              
 -27.2                0.29476              
 -27.4                0.31647              
 -27.6                0.33761              
 -27.8                0.3602               
 -28.                 0.39404              
 -28.2                0.43287              
 -28.4                0.46299              
 -28.6                0.48115              
 -28.8                0.50420              
 -29.                 0.52761              
 -29.2                0.53741              
 -29.4                0.54577              
 -29.6                0.54653              
 -29.8                0.54884              
 -30.                 0.54526              
 -30.2                0.52639              
 -30.4                0.50686              
 -30.6                0.49987              
 -30.8                0.45691              
 -31.                 0.42119              
 -31.2                0.38236              
 -31.4                0.34872              
 -31.6                0.32237              
 -31.8                0.28551              
 -32.                 0.24719              
 -32.2                0.21170              
 -32.4                0.18382              
 -32.6                0.15699              
 -32.8                0.12369              
 -33.                 0.09365              
 -33.2                0.07655              
 -33.4                0.07291              
 -33.6                0.06638              
 -33.8                0.05883              
 -34.                 0.04565              
 -34.2                0.03352              
 -34.4                0.02575              
 -34.6                0.02293              
 -34.8                0.02002              
 -35.                 0.01750              
 -35.2                0.01520              
 -35.4                0.01362              
 -35.6                0.01115              
 -35.8                0.00889              
 -36.                 0.00723              
 -36.2                0.00534              
 -36.4                0.00500              
 -36.6                0.00484              
 -36.8                0.00442              
 -37.                 0.00379              
 -37.2                0.00280              
 -37.4                0.00166              
 -37.6                0.00065              
 -37.8               -0.00100              
 -38                 -0.00254              
 -38.2               -0.00388              
 -38.4               -0.00425              
 -38.6               -0.00427              
 -38.8               -0.00519              
 -39                 -0.00552              
 -39.2               -0.00465              
 -39.4               -0.00417              
 -39.6               -0.00359              
 -39.8               -0.00284              
 -40                 -0.00202              
 -40.2               -0.00133              
 -40.4               -0.00148              
 -40.6               -0.00112              
 -40.8               -0.00024              
 -41.                 0.00075              
 -41.2                0.00144              
 -41.4                0.00142              
 -41.6                0.00147              
 -41.8                0.00123              
 -42.                 0.00021              
 -42.2               -0.00059              
 -42.4               -0.00118              
 -42.6               -0.00216              
 -42.8               -0.00289              
 -43.                -0.00337              
 -43.2               -0.00440              
 -43.4               -0.00537              
 -43.6               -0.00565              
 -43.8               -0.00492              
 -44.                -0.00418              
 -44.2               -0.00335              
 -44.4               -0.00276              
 -44.6               -0.00284              
 -44.8               -0.00281              
 -45.                -0.00286              
 -45.2               -0.00317              
 -45.4               -0.00396              
 -45.6               -0.00426              
 -45.8               -0.00424              
 -46.                -0.00425              
 -46.2               -0.00424              
 -46.4               -0.00427              
 -46.6               -0.00424              
 -46.8               -0.00340              
 -47.                -0.00276              
 -47.2               -0.00291              
 -47.4               -0.00252              
 -47.6               -0.00163              
 -47.8               -0.00064              
 -48.                 0.00003              
 -48.2                0.00000              
 -48.4                0.00002              
 -48.6                0.00001              
 -48.8                0.00001              
 -49.                 0.00001              
 -49.2                0.00002              
 -49.4                0.00047              
 -49.6                0.00256              
 -49.8                0.00381              
 -50.                 0.00481              
 -50.2                0.00617              
 -50.4                0.00750              
 -50.6                0.00921              
 -50.8                0.01162              
 -51.                 0.01294              
 -51.2                0.01266              
 -51.4                0.01340              
 -51.6                0.01510              
 -51.8                0.01638              
 -52.                 0.01709              
 -52.2                0.01835              
 -52.4                0.01932              
 -52.6                0.01917              
 -52.8                0.01937              
 -53.                 0.01985              
 -53.2                0.02019              
 -53.4                0.01991              
 -53.6                0.01916              
 -53.8                0.01930              
 -54.                 0.01875              
 -54.2                0.01673              
 -54.4                0.01510              
 -54.6                0.01448              
 -54.8                0.01341              
 -55.                 0.01192              
 -55.2                0.01097              
 -55.4                0.00937              
 -55.6                0.00847              
 -55.8                0.00858              
 -56.                 0.00855              
 -56.2                0.00854              
 -56.4                0.00796              
 -56.6                0.00674              
 -56.8                0.00639              
 -57.                 0.00638              
 -57.2                0.00573              
 -57.4                0.00499              
 -57.6                0.00419              
 -57.8                0.00324              
 -58.                 0.00127              
 -58.2                0.00008              
 -58.4                0.00002              
 -58.6                0.00000              
 -58.8                0.00002              
 -59.                -0.00007              
 -59.2               -0.00091              
 -59.4               -0.00201              
##END=
